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5-MeO-DALT analysis

5-MeO-DALT Analysis  24th January 2012


Our first test batch of 5-MeO-DALT was tested at 89% purity. Despite eventually being told by our experts that this was acceptable purity and in the expected zone for this particular compound (don't believe the 99.9% nonsense that we see elsewhere), BUT we still had it sent back the lab, and received back 98%+ material, which is exceptional quality for 5-MeO-DALT - the highest quality on the UK market.

 

Our independent expert scientist makes the following proffesional interpretation of the spectra:


"NMR: spectra is fine on id/purity: broad singlet at 10.6ppm = the typical indole NH, the large change to the earlier batch points to an hcl salt of this batch!! (right, its soluble in H2O?), the 4 indolearomatic H's are at 6,7-7.25ppm, those characteristic double bond hydrogens of the allyls "in the middle" at 5.1-5.25 and 5.8ppm, with 4 resp. 2 protons; the OCH3 singlet at 3.8ppm. The 2 CH2 of the ethyl indole side chain are at 2.75ppm plus the 2 H2 between the nitrogen and the double bonds, sharply at 3.2ppm. Two very minor solvent impurities prove that this is clearly a reworked/new sample.

 

But wait - on reflection, I have overlooked the DMSO information on their spectrum, so that small peak at 2.5ppm is actually not a solvent, but the beloved DMSO-d6 signal! Great! Very good quality DMSO-d6 then on their side (99.5D%?), very low HDO peak at 3.3. So I correct myself, its the freebase with only minor water content, very good practice on that NMR and compound, I'm very happy now with that labs work!"

 

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1H NMR:

 

5-MeO-DALT 1H NMR Spectrograph



 

 

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